Standard

ASTM D1238

ASTM D1238 is an American standard that specifies test methods for determining the melt flow rate (MFR) and melt volume rate (MVR) of thermoplastic materials using an extrusion plastometer.

ASTM D1238 provides guidelines on how to measure the flow properties of molten thermoplastic materials under specified temperature and load conditions. This test determines how easily a polymer flows when melted, which is critical for understanding processing behavior, material consistency, and quality control.

Purpose of ASTM D1238 Testing:

  • It establishes a consistent methodology for assessing the melt flow characteristics of thermoplastic materials using an extrusion plastometer.
  • The test involves heating a polymer sample in a heated barrel to a specified temperature, then forcing it through a standardized die using a weighted piston, measuring either the mass extruded in 10 minutes (MFR in g/10min) or the volume extruded (MVR in cm³/10min).
  • The melt flow rate indicates how easily the polymer flows when molten, with higher values indicating more fluid materials that flow easily (lower molecular weight), and lower values indicating more viscous materials that resist flow (higher molecular weight).
  • Different test conditions (temperature and load combinations like 190°C/2.16kg, 210°C/2.16kg, or 230°C/2.16kg) are specified for different polymer families to enable standardized comparisons.
  • Having a standardized test method ensures results are reproducible and comparable across different laboratories and manufacturers.

Application to 3D Printing Filament:

  • Many 3D printing filaments are thermoplastics (like PLA, ABS, PETG, and others). Understanding melt flow rate helps predict how the material will extrude through the printer's hotend and deposit onto the build plate.
  • Manufacturers can use ASTM D1238 testing to verify batch-to-batch consistency in their filament production, ensuring predictable extrusion behavior and preventing issues like inconsistent flow, poor layer adhesion, or nozzle clogging.
  • Designers and engineers might reference ASTM D1238 results to understand the processing window for a material, helping optimize print settings like temperature, print speed, and flow rate multipliers.
  • The standardized nature of ASTM D1238 testing helps in comparing different filament brands or formulations, ensuring that the material's flow behavior is predictable, which is especially important for achieving consistent print quality and troubleshooting extrusion problems.

Benefits for 3D Printing and End Users:

  • Quality Control: It allows filament producers to maintain consistent melt flow properties across production batches, ensuring predictable extrusion behavior and preventing print failures due to inconsistent material viscosity or molecular weight variations.
  • Material Selection: Users can review ASTM D1238 results (if available) to understand a filament's flow characteristics, helping them set appropriate print temperatures and speeds for optimal extrusion and layer bonding.
  • Predictable Performance: Understanding the melt flow rate helps predict how easily a filament will extrude, which affects layer adhesion, surface finish, bridging capability, stringing behavior, and the ability to print fine details or at higher speeds.

References

Read more about ASTM D1238 on ASTM's website.